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Nt Nitriding

Nitriding · Tratamiento térmico · ISO 1101 + ASME Y14.5

Example in plan

Nitride0.4mm·700-900HV

How to interpret it

On the drawing, “Nitride 0.4 mm · 700-900 HV” states a nitriding requirement.

What controls

Diffusion of nitrogen into the surface at a relatively low temperature, with no subsequent quench, which creates a very hard, wear-resistant layer with minimal distortion. Since there is no phase change or rapid cooling, the part barely moves, which allows already finished parts to be nitrided. The trade-off is that the layer is thin and does not tolerate generous grinding: removing a few hundredths can take away much of what was achieved. It only works well on steels with the appropriate alloying elements.

How to verify

Surface hardness with a low-load hardness tester or microhardness tester, because a high load punches through the layer and actually measures the core: this is the classic mistake when verifying nitriding. Case depth and white layer thickness are determined by metallography on a witness coupon from the same load, with a microhardness traverse from the surface. The heat treatment certificate must record the cycle, hardness and thicknesses.

Workshop guideline values

General
Case depths on the order of 0.2–0.4 mm on parts with moderate wear.
Accuracy
Case depths on the order of 0.3–0.6 mm with surface hardness specified in HV.
High precision
White layer controlled to a few microns and case depth certified per load.

Guidance only: the drawing's value always wins.

Common mistakes when interpreting it

  • Measuring the hardness of a nitrided part with the usual load of a Rockwell test: the indenter punches through the layer and the reading is invalid.
  • Grinding a nitrided part as if it had a carburized case: here, hundredths count.
  • Nitriding a steel that is not alloyed for it and expecting catalog hardness values.

How to get it in the workshop / if it comes out of tolerance

It is the treatment for parts that cannot distort: lead screws and spindles, molds, liners, precision shafts. The part is machined to final size, except for a light subsequent polish, and areas that must not harden are masked. Check that the steel is suitable for nitriding; on an ordinary steel the result is poor. Keep in mind that a very thin, brittle compound layer, the so-called white layer, usually forms on top of the diffusion zone, and the drawing may limit its maximum thickness.

Low measured hardness with correct case: almost always a method problem, from using too much load on the hardness tester; repeat with microhardness. White layer above the limit: cycle adjustment at the heat treater, or light subsequent polishing if the drawing allows. Spalling or flaking of the layer: excessive white layer or poorly prepared surface before nitriding. If grinding is needed afterward, it must be accounted for in the specified depth.

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